- CHARACTERIZATION OF KEY AROMA-ACTIVE TERPENES IN BRAZILIAN SEASONINGS USING ECO-FRIENDLY DI-SPME WITH GC×GC-MS AND ODOR ACTIVITY VALUE WORKFLOW
OLIVEIRA, JHONATAN BISPO DE ; Menezes, Helvécio Costa ; SOUZA, PATTERSON PATRÍCIO DE ; LOURDES CARDEAL, ZENILDA DE . Characterization of key aroma-active terpenes in Brazilian seasonings using eco-friendly DI-SPME with GC×GC-MS and odor activity value workflow. Npj Science Of Food, v. xx, p. xx, 2026.
http://dx.doi.org/10.1038/s41538-025-00687-2 - DI-SPME METHOD FOR THE ANALYSIS OF FIRE ACCELERANTS IN SIMULATED FIRE DEBRIS SAMPLES USING GC/MS AND GC×GC/Q-TOFMS
FIEL, WAGNER AUGUSTO ; LORDEIRO, ROGÉRIO ARAÚJO ; Cardeal, Zenida de Lourdes ; Menezes, Helvécio Costa . DI-SPME method for the analysis of fire accelerants in simulated fire debris samples using GC/MS and GC×GC/Q-TOFMS. TALANTA, v. 303, p. 129481, 2026.
http://dx.doi.org/10.1016/j.talanta.2026.129481 - COMPREHENSIVE SCREENING AND RISK ASSESSMENT OF PESTICIDE RESIDUES IN SPICES AND DRIED HERBS USING ECO-FRIENDLY MICROEXTRACTION AND GC×GC/MS
DE OLIVEIRA, JHONATAN BISPO ; Menezes, Helvécio Costa ; DE SOUZA, PATTERSON PATRÍCIO ; De Lourdes Cardeal, Zenilda . Comprehensive screening and risk assessment of pesticide residues in spices and dried herbs using eco-friendly microextraction and GC×GC/MS. MICROCHEMICAL JOURNAL, v. 227, p. 118889, 2026.
http://dx.doi.org/10.1016/j.microc.2026.118889 - DEVELOPMENT OF NEW PDMS IN TUBE EXTRACTION MICRODEVICE FOR ENHANCED MONITORING OF POLYCYCLIC AROMATIC HYDROCARBONS AND THEIR DERIVATIVES IN WATER
COELHO, NATHAN DE SOUZA ; Menezes, Helvécio Costa ; Cardeal, Zenilda de Lourdes . Development of new PDMS in tube extraction microdevice for enhanced monitoring of polycyclic aromatic hydrocarbons and their derivatives in water. TALANTA, v. 281, p. 126882, 2025.
http://dx.doi.org/10.1016/j.talanta.2024.126882 - ANALYSIS OF CONTAMINANTS IN SURFACE WATER AFTER THE COLLAPSE OF THE CÓRREGO DO FEIJÃO MINE DAM IN BRUMADINHO, BRAZIL
Menezes, Helvécio Costa ; ORLANDO, RICARDO MATHIAS ; Augusti, Rodinei ; DE MACEDO, ADRIANA NORI ; ALMEIDA, MARIANA RAMOS ; De Lourdes Cardeal, Zenilda ; VALENZUELA, EDUARD F. ; RIBEIRO, CYNTIA CABRAL ; AVELAR, MILLENA CHRISTIE FERREIRA ; DE FREITAS, MARINA CANESCHI ; DA SILVA, LUCAS PINTO ; GOMES, JOSÉ MESSIAS ; GOMES, JÚLIA CÉLIA LIMA ; AUGUSTI, JULIA VASCONCELLOS ; LOPES, BÁRBARA OLIVEIRA ; DE OLIVEIRA MELO, NATHALIA ; DA SILVA, LUCIENE PAIVA MOREIRA ; DE SOUSA, DENISE VERSIANE MONTEIRO . Analysis of contaminants in surface water after the collapse of the Córrego do Feijão mine dam in Brumadinho, Brazil. SCIENCE OF THE TOTAL ENVIRONMENT, v. 990, p. 179954, 2025.
http://dx.doi.org/10.1016/j.scitotenv.2025.179954 - ASSESSING PAH CONTAMINATION IN BRAZILIAN URBAN SOILS: ECO-FRIENDLY MICROEXTRACTION FOR SOURCE IDENTIFICATION AND RISK EVALUATION
Jhonatan Bispo de Oliveira ; Menezes, H.C. ; SOUZA, P. P. DE ; Cardeal, Zenilda L. . Assessing PAH contamination in Brazilian urban soils: Eco-friendly microextraction for source identification and risk evaluation. ENVIRONMENTAL POLLUTION, v. xxx, p. 126745, 2025.
http://dx.doi.org/10.1016/j.envpol.2025.126745 - GREEN MICROEXTRACTION AND GC-×-GC/MS QUANTIFICATION OF PAHS AND DERIVATIVES IN ROASTED/SMOKED SPICES AND DRY HERBS: IMPLICATIONS FOR FOOD SAFETY
DE OLIVEIRA, JHONATAN BISPO ; Menezes, Helvécio Costa ; DE SOUZA, PATTERSON PATRÍCIO ; De Lourdes Cardeal, Zenilda . Green microextraction and GC-×-GC/MS quantification of PAHs and derivatives in roasted/smoked spices and dry herbs: implications for food safety. FOOD CHEMISTRY, v. 495, p. 146655, 2025.
http://dx.doi.org/10.1016/j.foodchem.2025.146655 - IMPACT OF EXPOSURE TO ATMOSPHERIC PARTICULATE MATTER IN HUMAN SKIN-DERIVED FIBROBLAST CELLS: A METABOLOMICS APPROACH FOR THE CLASS OF AMINO ACIDS BASED ON GC×GC-Q-TOFMS/MS
RODRIGUES, SAMANTHA C.H. ; Menezes, Helvécio C. ; GOMES, DAWIDSON A. ; Cardeal, Zenilda L. . Impact of exposure to atmospheric particulate matter in human skin-derived fibroblast cells: A metabolomics approach for the class of amino acids based on GC×GC-Q-TOFMS/MS. JOURNAL OF HAZARDOUS MATERIALS, v. 461, p. 132606-1322613, 2024.
http://dx.doi.org/10.1016/j.jhazmat.2023.132606 - DEVELOPMENT AND APPLICATION OF NOVEL EXTRACTION METHOD TO ANALYZE HERBAL SUPPLEMENTS AND ADULTERANT DETERMINATION BY GCxGC/Q-TOFMS
DE OLIVEIRA, JHONATAN BISPO ; CARVALHO, MARIA FERNANDA MENDES ; DE SOUZA, PATTERSON PATRÍCIO ; De Lourdes Cardeal, Zenilda . Development and Application of Novel Extraction Method to Analyze Herbal Supplements and Adulterant Determination by GCxGC/Q-TOFMS. Food Analytical Methods, v. 17, p. 1267, 2024.
http://dx.doi.org/10.1007/s12161-024-02657-y - AN EXPLORATORY STUDY OF VOLATILE AND SEMI-VOLATILE ORGANIC COMPOUNDS IN PM2.5 ATMOSPHERIC PARTICLES FROM AN OUTDOOR ENVIRONMENT IN BRAZIL
BATISTA, JOSIMAR M. ; VALENZUELA, EDUARD F. ; Menezes, Helvécio C. ; Cardeal, Zenilda L. . An exploratory study of volatile and semi-volatile organic compounds in PM2.5 atmospheric particles from an outdoor environment in Brazil. Environmental Science and Pollution Research, v. 14, p. 120-128, 2024.
http://dx.doi.org/10.1007/s11356-024-35647-y - A BIOMARKERS STUDY OF HUMAN SKIN FIBROBLASTS EXPOSITION TO GLYPHOSATEBASED HERBICIDE USING AN UNTARGETED AND TARGETED METABOLOMICS APPROACH
BATISTA, JOSIMAR M. ; GOMES, DAWIDSON A. ; ARMIJOS, M. J. ; RODRIGUES, M. A. ; Menezes, H.C. ; Cardeal, Zenilda L. . A biomarkers study of human skin fibroblasts exposition to glyphosatebased herbicide using an untargeted and targeted metabolomics approach. Chemosphere, v. 370, p. 143998, 2024.
http://dx.doi.org/10.1016/j.chemosphere.2024.143998 - VOLATILOME STUDY OF JABUTICABA ( PLINIA CAULIFLORA ) USING A HYDROPHILIC MICROPOROUS CARTRIDGE WITH DIRECT IMMERSION SOLID PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY SYSTEM WITH A HYBRID QUADRUPOLE TIME-OF-FLIGHT MASS SPECTROMETRY
DE OLIVEIRA, JHONATAN BISPO ; RODRIGUES, SAMANTHA CHRISTINA ; Menezes, Helvécio Costa ; DE SOUZA, PATTERSON PATRÍCIO ; Cardeal, Zenilda de Lourdes . Volatilome Study of Jabuticaba ( Plinia cauliflora ) Using a Hydrophilic Microporous Cartridge with Direct Immersion Solid Phase Microextraction and Gas Chromatography System With a Hybrid Quadrupole Time-Of-Flight Mass Spectrometry. JOURNAL OF SEPARATION SCIENCE, v. 47, p. 1-9, 2024.
http://dx.doi.org/10.1002/jssc.70038 - ENDOPHYTIC SPECIES OF INDURATIA FROM COFFEE AND CARQUEJA PLANTS FROM BRAZIL AND ITS POTENTIAL FOR THE BIOLOGICAL CONTROL OF TOXICOGENIC FUNGI ON COFFEE BEANS BY MEANS OF ANTIMICROBIAL VOLATILES
GOMES, ANDRÉ ANGELO MEDEIROS ; PAES, SIMONE ALBINO ; FERREIRA, ANA PAULA SATO ; PINHO, DANILO BATISTA ; De Lourdes Cardeal, Zenilda ; Menezes, Helvécio Costa ; CARDOSO, PATRÍCIA GOMES ; PEREIRA, OLINTO LIPARINI . Endophytic species of Induratia from coffee and carqueja plants from Brazil and its potential for the biological control of toxicogenic fungi on coffee beans by means of antimicrobial volatiles. BRAZILIAN JOURNAL OF MICROBIOLOGY, v. xx, p. 01, 2023.
http://dx.doi.org/10.1007/s42770-022-00887-y - STRATEGIES FOR METABOLOMIC ANALYSIS OF DAMAGED SKIN FROM CELL AND TISSUE SAMPLES USING GAS CHROMATOGRAPHY-MASS SPECTROMETRY
RODRIGUES, SAMANTHA ; MENEZES, HELVÉCIO ; GOMES, DAWIDSON ; CARDEAL, ZENILDA . Strategies for Metabolomic Analysis of Damaged Skin from Cell and Tissue Samples Using Gas Chromatography-Mass Spectrometry. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, v. xxx, p. 01, 2023.
http://dx.doi.org/10.21577/0103-5053.20230005 - DEVELOPMENT OF A SIMPLE INTEGRATIVE CARBON NANOMATERIAL MICROEXTRACTION METHOD WITH GC-MS FOR ASSESSING PESTICIDE RESIDUES IN APPLES
VALENZUELA, EDUARD F. ; ANDRÉ, LEILIANE C. ; MENEZES, HELVECIO C. ; Cardeal, Zenilda L. . Development of a Simple Integrative Carbon Nanomaterial Microextraction Method with GC-MS for Assessing Pesticide Residues in Apples. Journal of Chemistry, v. 2023, p. 1-14, 2023.
http://dx.doi.org/10.1155/2023/5561490 - DEVELOPMENT OF POLYPROPYLENE MEMBRANES GRAFTED WITH NANOCELLULOSE TO ANALYZE ORGANIC POLLUTANTS IN ENVIRONMENTAL WATERS USING MINIATURIZED PASSIVE SAMPLERS BASED ON LIQUID-PHASE MICROEXTRACTION
MINHO, LUCAS ALMIR CAVALCANTE ; De Lourdes Cardeal, Zenilda ; Menezes, Helvécio Costa . Development of polypropylene membranes grafted with nanocellulose to analyze organic pollutants in environmental waters using miniaturized passive samplers based on liquid-phase microextraction. MICROCHEMICAL JOURNAL, v. 190, p. 108641, 2023.
http://dx.doi.org/10.1016/j.microc.2023.108641 - A DEEP LEARNING-BASED SIMULATOR FOR COMPREHENSIVE TWO-DIMENSIONAL GC APPLICATIONS
MINHO, LUCAS ALMIR CAVALCANTE ; Cardeal, Zenilda de Lourdes ; Menezes, Helvécio Costa . A deep learning-based simulator for comprehensive two-dimensional GC applications. JOURNAL OF SEPARATION SCIENCE, v. xxx, p. 1-10, 2023.
http://dx.doi.org/10.1002/jssc.202300187 - EFFECTS OF BISPHENOL A ON MURINE SALIVARY GLANDS AND HUMAN TUMOR CELL LINES
SILVA, GABRIELA KELLY DA ; DE ARRUDA, JOSÉ ALCIDES ALMEIDA ; ALMEIDA, TATIANA FERNANDES ARAÚJO ; OLIVEIRA, SICÍLIA REZENDE ; ROCHA, PAULA ALVES DA SILVA ; MESQUITA, RICARDO ALVES ; Cardeal, Zenilda de Lourdes ; Menezes, Helvécio Costa ; DINIZ, IVANA MÁRCIA ALVES ; MACARI, SORAIA ; LEOPOLDINO, ANDRÉIA MACHADO ; SILVA, TARCÍLIA APARECIDA . Effects of bisphenol A on murine salivary glands and human tumor cell lines. EXPERIMENTAL AND MOLECULAR PATHOLOGY, v. 134, p. 104870, 2023.
http://dx.doi.org/10.1016/j.yexmp.2023.104870 - DETERMINATION OF PESTICIDE RESIDUE IN MARGINAL LAGOONS OF NATURAL PARKS IN BRAZIL USING AN IMPROVED CALIBRATE PASSIVE SAMPLER
VALENZUELA, EDUARD F. ; MINHO, LUCAS A.C. ; Menezes, Helvécio C. ; Cardeal, Zenilda L. . Determination of pesticide residue in marginal lagoons of natural parks in Brazil using an improved calibrate passive sampler. SCIENCE OF THE TOTAL ENVIRONMENT, v. xxx, p. 168003, 2023.
http://dx.doi.org/10.1016/j.scitotenv.2023.168003 - MITIGATING MATRIX EFFECTS IN GROUNDWATER: A SIMPLE AND VERSATILE METHOD FOR QUANTIFYING CONTAMINANTS IN GROUNDWATER USING ONLINE SPE-UHPLC-MS/MS
ORLANDO, RICARDO MATHIAS ; Augusti, Rodinei ; NORI DE MACEDO, ADRIANA ; ALMEIDA, MARIANA RAMOS ; Cardeal, Zenilda de Lourdes ; Menezes, Helvécio C. ; WINDMOELLER, CLAUDIA CARVALHINHO ; RIBEIRO, CYNTIA CABRAL ; AVELAR, MILLENA CHRISTIE FERREIRA ; DE FREITAS, MARINA CANESCHI ; DA SILVA, LUCAS PINTO ; GOMES, JOSÉ MESSIAS ; GOMES, JÚLIA CÉLIA LIMA ; AUGUSTI, JULIA VASCONCELLOS ; LOPES, BÁRBARA OLIVEIRA ; MELO, NATHALIA DE OLIVEIRA ; MOREIRA DA SILVA, LUCIENE PAIVA ; DE SOUSA, DENISE VERSIANE MONTEIRO . Mitigating Matrix Effects in Groundwater: A Simple and Versatile Method for Quantifying Contaminants in Groundwater Using Online SPE-UHPLC-MS/MS. Acs Es&T Water, v. 3, p. 3941-3951, 2023.
http://dx.doi.org/10.1021/acsestwater.3c00376 - NOVEL MINIATURIZED PASSIVE SAMPLING DEVICES BASED ON LIQUID PHASE MICROEXTRACTION EQUIPPED WITH CELLULOSE-GRAFTED MEMBRANES FOR THE ENVIRONMENTAL MONITORING OF PHTHALIC ACID ESTERS IN NATURAL WATERS.
MINHO, LUCAS A.CAVALCANTE ; VALENZUELA, EDUARD F. ; Cardeal, Zenilda de L. ; Menezes, Helvécio C. . Novel miniaturized passive sampling devices based on liquid phase microextraction equipped with cellulose-grafted membranes for the environmental monitoring of phthalic acid esters in natural waters. ANALYTICA CHIMICA ACTA, v. xx, p. 340405, 2022.
http://dx.doi.org/10.1016/j.aca.2022.340405 - ASSESSMENT OF POLYCYCLIC AROMATIC HYDROCARBONS AND DERIVATIVES IN BEER USING A NEW COLD FIBER-SOLID PHASE MICROEXTRACTION SYSTEM.
RESENDE DOS SANTOS, ROSIMEIRE; ORLANDO, RICARDO MATHIAS; DE LOURDES CARDEAL, ZENILDA; MENEZES, HELVÉCIO COSTA . Assessment of Polycyclic Aromatic Hydrocarbons and derivatives in beer using a new cold fiber-solid phase microextraction system. FOOD CONTROL, v. 126, p. 108104, 2021.
https://doi.org/10.1016/j.foodcont.2021.108104 - ASSESSMENT OF POLYCYCLIC AROMATIC HYDROCARBONS FROM INDUSTRIAL STACK EMISSIONS IN A BRAZILIAN URBAN ÁREA.
SANTOS, ROSIMEIRE R. ; MENEZES, HELVÉCIO C. ; CARDEAL, ZENILDA L.. Assessment of polycyclic aromatic hydrocarbons from industrial stack emissions in a Brazilian urban area. INTERNATIONAL JOURNAL OF ENVIRONMENTAL STUDIES, v. 2021, p. 1-13, 2021.
https://doi.org/10.1080/00207233.2021.1972660 - PHASE DISTRIBUTION OF POLYCYCLIC AROMATIC HYDROCARBONS AND THEIR OXYGENATED AND NITRATED DERIVATIVES IN THE AMBIENT AIR OF A BRAZILIAN URBAN ÁREA.
DOS SANTOS, ROSIMEIRE RESENDE ; CARDEAL, ZENILDA DE LOURDES ; MENEZES, HELVÉCIO COSTA . Phase distribution of polycyclic aromatic hydrocarbons and their oxygenated and nitrated derivatives in the ambient air of a Brazilian urban area. CHEMOSPHERE, v. 250, p. 126223, 2020.
https://doi.org/10.1016/j.chemosphere.2020.126223 - METABOLOMIC STUDIES OF AMINO ACID ANALYSIS IN SACCHAROMYCES CELLS EXPOSED TO SELENIUM AND GAMMA IRRADIATION.
BATISTA, JOSIMAR M. ; NEVES, MARIA J. ; PEREIRA, ALLINE G. ; GONÇALVES, LETÍCIA S. ; MENEZES, HELVÉCIO C. ; CARDEAL, ZENILDA L.. Metabolomic studies of amino acid analysis in Saccharomyces cells exposed to selenium and gamma irradiation. ANALYTICAL BIOCHEMISTRY, v. 597, p. 113666, 2020.
https://doi.org/10.1016/j.ab.2020.113666 - PASSIVE AND GRAB SAMPLING METHODS TO ASSESS PESTICIDE RESIDUES IN WATER. A REVIEW.
VALENZUELA, EDUARD F. ; MENEZES, HELVÉCIO C. ; CARDEAL, ZENILDA L.. Passive and grab sampling methods to assess pesticide residues in water. A review. Environmental Chemistry Letters, v. 18, p. 1019-1048, 2020.
https://doi.org/10.1007/s10311-020-00998-8 - A NEW CARBON NANOMATERIAL SOLID-PHASE MICROEXTRACTION TO PRE-CONCENTRATE AND EXTRACT PESTICIDES IN ENVIRONMENTAL WATER.
VALENZUELA, EDUARD F. ; DE PAULA, FABIANO G.F. ; TEIXEIRA, ANA PAULA C. ; MENEZES, HELVÉCIO C. ; CARDEAL, ZENILDA L.. A new carbon nanomaterial solid-phase microextraction to pre-concentrate and extract pesticides in environmental water. TALANTA, v. 217, p. 121011, 2020.
https://doi.org/10.1016/j.talanta.2020.121011 - SALIVA BIOMONITORING USING LPME-GC/MS METHOD TO ASSESS DENTISTRY EXPOSURE TO PLASTICIZERS.
GOMES, JOSÉ MESSIAS ; ALMEIDA, TATIANA FERNANDES ARAUJO ; DA SILVA, TARCÍLIA APARECIDA ; DE LOURDES CARDEAL, ZENILDA ; MENEZES, HELVÉCIO COSTA . Saliva biomonitoring using LPME-GC/MS method to assess dentistry exposure to plasticizers. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, v. 412, p. 7799-7810, 2020.
https://doi.org/10.1007/s00216-020-02908-x
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GOMES, ANDRÉ ANGELO MEDEIROS ; PAES, SIMONE ALBINO ; FERREIRA, ANA PAULA SATO ; PINHO, DANILO BATISTA ; DE LOURDES CARDEAL, ZENILDA ; Menezes, Helvécio Costa ; CARDOSO, PATRÍCIA GOMES ; PEREIRA, OLINTO LIPARINI . Endophytic species of Induratia from coffee and carqueja plants from Brazil and its potential for the biological control of toxicogenic fungi on coffee beans by means of antimicrobial volatiles. BRAZILIAN JOURNAL OF MICROBIOLOGY, v. 53, p. 1, 2023. https://doi.org/10.1007/s42770-022-00887-y
- STRATEGIES FOR METABOLOMIC ANALYSIS OF DAMAGED SKIN FROM CELL AND TISSUE SAMPLES USING GAS CHROMATOGRAPHY-MASS SPECTROMETRY
RODRIGUES, SAMANTHA ; MENEZES, HELVÉCIO ; GOMES, DAWIDSON ; CARDEAL, ZENILDA . Strategies for Metabolomic Analysis of Damaged Skin from Cell and Tissue Samples Using Gas Chromatography-Mass Spectrometry. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, v. 1, p. 1-14, 2023. https://dx.doi.org/10.21577/0103-5053.20230005
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MINHO, LUCAS A.CAVALCANTE ; VALENZUELA, EDUARD F. ; CARDEAL, ZENILDA DE L. ; Menezes, Helvécio C. . Novel miniaturized passive sampling devices based on liquid phase microextraction equipped with cellulose-grafted membranes for the environmental monitoring of phthalic acid esters in natural waters. ANALYTICA CHIMICA ACTA, v. 1231, p. 340405, 2022.
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- CANCER RISK ASSESSMENT AND SOURCE APPORTIONMENT OF THE GAS- AND PARTICULATE-PHASE OF THE POLYCYCLIC AROMATIC HYDROCARBONS IN A METROPOLITAN REGION IN BRAZIL
GALVÃO, ELSON SILVA ; PAIVA, HENRIQUE BITTENCOURT ; Menezes, Helvécio Costa ; DE ALMEIDA ALBUQUERQUE, TACIANA TOLEDO ; Cardeal, Zenilda de Lourdes . Cancer risk assessment and source apportionment of the gas- and particulate-phase of the polycyclic aromatic hydrocarbons in a metropolitan region in Brazil. CHEMOSPHERE, v. 311, p. 136872-136883, 2022. https://doi.org/10.1016/j.chemosphere.2022.136872
- EVALUATION OF AMINO ACID PROFILE BY TARGETED METABOLOMICS IN THE EUKARYOTIC MODEL UNDER EXPOSURE OF BENZO[A]PYRENE AS THE EXCLUSIVE STRESSOR
Josimar M. Batista, Maria J. Neves, Helvécio C. Menezes, Zenilda L. Cardeal, Evaluation of amino acid profile by targeted metabolomics in the eukaryotic model under exposure of benzo[a]pyrene as the exclusive stressor, Talanta, Volume 265, 2023, 124859, ISSN 0039-9140,
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